2-Morpholin-4-yl-5-nitro-benzoyl chloride → HCID 11676078, compound

HRID 1723637Notes

Reaction equation

HRID 1723637 reaction equation
[N:1]1([C:7]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:8]=2[C:9](Cl)=[O:10])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[NH:19]1[CH2:24][CH:23]=[C:22]([C:25]2[CH:32]=[CH:31][C:28]([C:29]#[N:30])=[CH:27][CH:26]=2)[CH2:21][CH2:20]1>>[N:1]1([C:7]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:8]=2[C:9]([N:19]2[CH2:20][CH:21]=[C:22]([C:25]3[CH:32]=[CH:31][C:28]([C:29]#[N:30])=[CH:27][CH:26]=3)[CH2:23][CH2:24]2)=[O:10])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 172741532-Morpholin-4-yl-5-nitro-benzoyl chlorideHCID 67376604HCID 67376604, compound

Product 1

HCID 11676078HCID 11676078, compound

Procedure

According to the procedure described for the synthesis of example 1, the title compound has been synthesized from 2-morpholin-4-yl-5-nitro-benzoyl chloride and 4-(1,2,3,6-Tetrahydro-pyridin-4-yl)-benzonitrile (CAS: 460365-22-4). MS (m/e): 417.0 (M−H, 100%)

Workup

  1. customdescribed for the synthesis of example 1

Sources & evidence

ORD record
ord-01f965e2aae64f239953019f5b62f8c2
Source dataset
uspto-grants-2009_02
Patent number
US07485637B2

Reaction notes

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