2-Morpholino-5-nitrobenzoic acid → HCID 11684259, compound

HRID 1723646Notes

Reaction equation

HRID 1723646 reaction equation
[N:1]1([C:7]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:8]=2[C:9]([OH:11])=O)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[CH3:19][S:20]([C:23]1[CH:28]=[CH:27][C:26]([C:29]2[CH2:30][CH2:31][NH:32][CH2:33][CH:34]=2)=[CH:25][CH:24]=1)(=[O:22])=[O:21]>>[CH3:19][S:20]([C:23]1[CH:24]=[CH:25][C:26]([C:29]2[CH2:34][CH2:33][N:32]([C:9]([C:8]3[CH:12]=[C:13]([N+:16]([O-:18])=[O:17])[CH:14]=[CH:15][C:7]=3[N:1]3[CH2:2][CH2:3][O:4][CH2:5][CH2:6]3)=[O:11])[CH2:31][CH:30]=2)=[CH:27][CH:28]=1)(=[O:22])=[O:21]

Participants

3

Reactant 2

HCID 27257552-Morpholino-5-nitrobenzoic acidHCID 68978456HCID 68978456, compound

Product 1

HCID 11684259HCID 11684259, compound

Procedure

According to the procedure described for the synthesis of example 4, step f, the title compound has been synthesized from 2-Morpholin-4-yl-5-nitro-benzoic acid and 4-(4-Methanesulfonyl-phenyl)-1,2,3,6-tetrahydro-pyridine. MS (m/e): 470.1 (M−H, 100%)

Workup

  1. customdescribed for the synthesis of example 4, step f

Sources & evidence

ORD record
ord-f1fdb6e54e1b44aabe78519daca2f998
Source dataset
uspto-grants-2009_02
Patent number
US07485637B2

Reaction notes

Loading…