2-Isopropoxy-5-methylsulfonylbenzoic acid → HCID 11655903, compound

HRID 1723648Notes

Reaction equation

HRID 1723648 reaction equation
[CH:1]([O:4][C:5]1[CH:13]=[CH:12][C:11]([S:14]([CH3:17])(=[O:16])=[O:15])=[CH:10][C:6]=1[C:7]([OH:9])=O)([CH3:3])[CH3:2].[CH3:18][S:19]([C:22]1[CH:27]=[CH:26][C:25]([C:28]2[CH2:29][CH2:30][NH:31][CH2:32][CH:33]=2)=[CH:24][CH:23]=1)(=[O:21])=[O:20]>>[CH:1]([O:4][C:5]1[CH:13]=[CH:12][C:11]([S:14]([CH3:17])(=[O:16])=[O:15])=[CH:10][C:6]=1[C:7]([N:31]1[CH2:30][CH:29]=[C:28]([C:25]2[CH:26]=[CH:27][C:22]([S:19]([CH3:18])(=[O:21])=[O:20])=[CH:23][CH:24]=2)[CH2:33][CH2:32]1)=[O:9])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acidHCID 68978456HCID 68978456, compound

Product 1

HCID 11655903HCID 11655903, compound

Procedure

According to the procedure described for the synthesis of example 4, step f, the title compound has been synthesized 2-isopropoxy-5-methanesulfonyl-benzoic acid and 4-(4-Methanesulfonyl-phenyl)-1,2,3,6-tetrahydro-pyridine. MS (m/e): 495.4 (M+NH4+, 100%)

Workup

  1. customdescribed for the synthesis of example 4, step f

Sources & evidence

ORD record
ord-b3168982d8dc4e12b12d7ed750d9ec29
Source dataset
uspto-grants-2009_02
Patent number
US07485637B2

Reaction notes

Loading…