2-Cyclopentyloxy-5-methanesulfonyl-benzoic acid → HCID 11641895, compound
Reaction equation
[CH:1]1([O:6][C:7]2[CH:15]=[CH:14][C:13]([S:16]([CH3:19])(=[O:18])=[O:17])=[CH:12][C:8]=2[C:9]([OH:11])=O)[CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:20][S:21]([C:24]1[CH:29]=[CH:28][C:27]([C:30]2[CH2:31][CH2:32][NH:33][CH2:34][CH:35]=2)=[CH:26][CH:25]=1)(=[O:23])=[O:22]>>[CH:1]1([O:6][C:7]2[CH:15]=[CH:14][C:13]([S:16]([CH3:19])(=[O:18])=[O:17])=[CH:12][C:8]=2[C:9]([N:33]2[CH2:32][CH:31]=[C:30]([C:27]3[CH:28]=[CH:29][C:24]([S:21]([CH3:20])(=[O:23])=[O:22])=[CH:25][CH:26]=3)[CH2:35][CH2:34]2)=[O:11])[CH2:2][CH2:3][CH2:4][CH2:5]1Participants
3
Procedure
According to the procedure described for the synthesis of example 4, step f, the title compound has been synthesized from 2-cyclopentyloxy-5-methanesulfonyl-benzoic acid and 4-(4-Methanesulfonyl-phenyl)-1,2,3,6-tetrahydro-pyridine. MS (m/e): 503.9 (M+, 100%)
Workup
- customdescribed for the synthesis of example 4, step f
Sources & evidence
- ORD record
- ord-269b625e994b426db22386ba5f18cfb7
- Source dataset
- uspto-grants-2009_02
- Patent number
- US07485637B2
Reaction notes
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