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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1723734Generated: October 31, 2026

4-Fluorobenzoyl chloride → HCID 57559107, compound

https://huagongshe.com/reaction/1723734

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Fluorobenzoyl chlorideHCID 67879—
ReactantEthyl 9-fluoro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylateHCID 66640204—
ProductHCID 57559107HCID 57559107—

Reaction Steps

The title compound was prepared in a manner similar to that described in Example 2 by using ethyl 9-fluoro-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate and 4-fluorobenzoyl chloride; 1H-NMR (CDCl3): δ 10.57 (1H, br s), 8.04 (1H, s), 7.62 (2H, dd), 7.29 (1H, m), 7.16 (3H, m), 6.95 (1H, m), 4.24 (4H, m), 3.20 (2H, m), 1.22 (3H, t); MS (ES): 397 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07485634B2
Source datasetuspto-grants-2009_02
ORD IDord-3fdeb15d786049fb9e9d58f57d7819c5
Source noteuspto-grants-2009_02