Tributylstannane → HCID 11557869, compound

Participants

Reaction Steps

The reaction is carried out according to the procedure for the preparation of 1f starting from 2b (68 mg, 0.18 mmol), AIBN (26 mg, 0.16 mmol), and tributyltin hydride (176 μl, 0.63 mmol) in tetrahydrofuran (THF) (10 ml). After a 2 h reflux followed by isolation and purification as described in Example 6, pure 2c crystallized from THF in two crops as a white solid.

Provenance & Evidence