HRID1724724

反应详情

EQUATION

反应方程式

HRID 1724724 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1,1-diphenyl-4-bromobutene (10.0 g) is dissolved in absolute ethanol (100 ml) and palladium on carbon (400 mg) is added. The reaction mixture is placed under hydrogen atmosphere (P=3.3 bar) for 6 hours. The mixture is filtered on kelite, the filtrate is concentrated to obtain the desired product as an orange oil (9.24 g).

WORKUP

后处理

  1. customfor 6 hours
  2. filtrationThe mixture is filtered on kelite
  3. concentrationthe filtrate is concentrated