HRID1724915

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68526

1-Bromo-2-phenoxyethane

C8H9BrO

反应SMILES：OC(c1cccs1)(c1cccs1)C12CCN(CC1)CC2

HCID68865599

1-Azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol

C16H19NOS2

PRODUCTS

产物

反应SMILES：OC(c1cccs1)(c1cccs1)C12CC[N+](CCOc3ccccc3)(CC1)CC2.[Br-]

HCID11713139

未命名化合物

收率 74.7%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol (0.0693 g, 0.227 mmol) and 2-bromoethyl phenyl ether (0.056 g, 0.279 mmol) in 1 MeOH/1 CHCl3 (3.0 mL) were reacted to give the desired product (0.0822 g, 74.7%). EI-MS m/z 426(M+) Rt (2.00 min).

WORKUP

后处理

customwere reacted