HRID1724916

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68522

Benzene, (3-bromopropoxy)-

C9H11BrO

反应SMILES：OC(c1cccs1)(c1cccs1)C12CCN(CC1)CC2

HCID68865599

1-Azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol

C16H19NOS2

PRODUCTS

产物

反应SMILES：OC(c1cccs1)(c1cccs1)C12CC[N+](CCCOc3ccccc3)(CC1)CC2.[Br-]

HCID11504564

未命名化合物

收率 45.5%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol (0.0578 g, 0.189 mmol) and 3-bromopropyl phenyl ether (0.033 mL, 0.209 mmol) in 1 MeOH/1 CHCl3 (4.0 mL) were reacted to give the desired product (0.0448 g, 45.4%). EI-MS m/z 440(M+) Rt (1.94 min).

WORKUP

后处理

customwere reacted