HRID1724918

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12503

(3-Bromopropyl)benzene

C9H11Br

反应SMILES：OC(c1cccs1)(c1cccs1)C12CCN(CC1)CC2

HCID68865599

1-Azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol

C16H19NOS2

PRODUCTS

产物

反应SMILES：OC(c1cccs1)(c1cccs1)C12CC[N+](CCCc3ccccc3)(CC1)CC2.[Br-]

HCID68960601

未命名化合物

收率 62.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol (0.0688 g, 0.225 mmol) and (3-bromopropyl)benzene (0.070 mL, 0.460 mmol) in 1 MeOH/1 CHCl3 (4.0 mL) were reacted to give the desired product (0.0685 g, 62.3%). EI-MS m/z 424(M+) Rt (1.97 min).

WORKUP

后处理

customwere reacted