HRID1725082

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID29625

2-Bromobenzyl cyanide

C8H6BrN

HCID10987806

(4,4-Dimethyl-2-oxo-1,4-dihydro-2H-3,1-benzoxazin-6-yl)boronic acid

C10H12BNO4

PRODUCTS

生成物

结构：CC1(C)OC(=O)Nc2ccc(-c3ccccc3CC#N)cc21

HCID23509611

未命名化合物

PROCEDURE

实验过程

Prepared according to procedure B from 2-bromophenylacetonitrile and (1,4-dihydro-4,4-dimethyl-2-oxo-2H-3,1-benzoxazin-6-yl)boronic acid. White solid; mp 176-179° C.; 1H-NMR (DMSO-d6), δ 10.31 (s, 1H), 7.53 (m, 1H), 7.48 (m,2H), 7.22-7.32 (m,3H), 6.98 (d,1H; J=8.0 Hz), 3.90 (s,2H), 1.64 (s,6H). MS (+)APCI [M+H]+ m/z=293. Anal. Calc. For C18H16N2O2: C, 73.95; H, 5.52; N, 9.58. Found: C, 73.51; H, 5.70; N, 9.39.

WORKUP

后处理

customPrepared