HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-D-Tyr(Me)-L-Ile-DL-Pip-OBzl → Boc-D-Tyr(Me)-L-Ile-DL-Pip-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-D-Tyr(Me)-L-Ile-DL-Pip-OBzl | HCID 131727274 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Boc-D-Tyr(Me)-L-Ile-DL-Pip-OH | HCID 131727273 | — |
Reaction Steps
Boc-D-Tyr(Me)-L-Ile-DL-Pip-OBzl (3.46 g, 7.37 mmol) was dissolved in methanol (30 ml) and subjected to catalytic hydrogenation in the presence of the 5% Pd-C (230 mg). After 8 hours, the catalyst Pd-C was filtered and the reaction solution was evaporated to obtain Boc-D-Tyr(Me)-L-Ile-DL-Pip-OH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488712B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-ef4820104077411bb43df8ebc1528af5 |
| Source note | uspto-grants-2009_02 |