HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl → Boc-D-Tyr(Me)-L-Ile-D-Pro-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl | HCID 58726683 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Boc-D-Tyr(Me)-L-Ile-D-Pro-OH | HCID 131723245 | — |
Reaction Steps
Boc-D-Tyr(Me)-L-Ile-D-Pro-OBzl (1.01 g, 1.70 mmol) was dissolved in methanol (20 ml) and subjected to catalytic hydrogenation in the presence of 5% Pd-C (150 mg). After 8 hours, the catalyst Pd-C was filtered and the reaction solution was evaporated to obtain Boc-D-Tyr(Me)-L-Ile-D-Pro-OH.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488712B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-97e51d78aeaf4d72b72fab877e9a9976 |
| Source note | uspto-grants-2009_02 |