HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 135421235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 136056013 | HCID 136056013 | — |
| Product | HCID 135421235 | HCID 135421235 | 16.1% |
Reaction Steps
Crude 8-chloro-11-methylsulfanyl-5H-dibenzo[b,e][1,4]diazepine (166JO50) (90 mg, purity 50%, 0.218 mmol) and morpholine (38 mg, 0.44 mmol) were reacted as described for Example 62 to give 11 mg of the title compound (166JO69B). MS (ESI) 314 (MH+). Purity for MH+ (UV/MS) 100/98.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07491715B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-b6dd4732f10244bcbd883278357dc679 |
| Source note | uspto-grants-2009_02 |