Pyridine → HCID 87605495, compound

Participants

Reaction Steps

A solution of Example 615C (288 mg, 0.66 mmol), methanesulfonyl chloride (188 mg, 1.64 mmol) and pyridine (104 mg, 1.32 mmol) in dichloromethane (5 mL) was stirred at ambient temperature overnight. Dichloromethane (20 mL) was added and the solution was washed with 1N HCl (2×10 mL) and brine (2×10 mL). The solution was then dried (MgSO4), filtered, and concentrated to provide the desired product (0.33 g, 97%).

Provenance & Evidence