Methanol → HCID 68970622, compound

Participants

Reaction Conditions

Reaction Steps

To solution of the above sulfide (1.2 g, 3.58 mmol) in MeOH (58 mL) cooled to 0° C. was added OXONE® (4.40 g, 7.15 mmol) and the mixture was stirred at 0° C. for 4 hours to afford 4-(4-methanesulfonyl-benzoyl)-piperidine-1-carboxylic acid tert-butyl ester as a white solid (802 mg, 61%) after basic work-up and purification.

Provenance & Evidence