HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 131726612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,5,8,11-Tetraoxatridecan-13-oic acid | HCID 9859324 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Product | HCID 131726612 | HCID 131726612 | 99% |
Reaction Steps
(CH3(OCH2CH2)3CH2OCH2COCl) was prepared according to Procedure 1. Oxalyl chloride (3.6 mL, 0.041 mol); {2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-acetic acid (3.3 g, 0.15 mol); pyridine (0.1 mL, 1 mmol) and anhydrous toluene (10 mL) to give CH3(OCH2CH2)3CH2OCH2COCl as yellow oil (3.5 g, 99%). This compound was used without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07494714B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-f42d3312c824451a8b016f87bc8e6c68 |
| Source note | uspto-grants-2009_02 |