HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentyl methyl ether → 2-Isopropenyl-1,3,5-trimethylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentyl methyl ether | HCID 138539 | — |
| Reactant | 2-(2,4,6-Trimethylphenyl)propan-2-ol | HCID 293003 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Isopropenyl-1,3,5-trimethylbenzene | HCID 518986 | 66.8% |
Reaction Steps
The same experiment as in Example 4 was carried out, except for using a mixed solvent of CPME and THF (1:1 by volume) instead of 50 ml of CPME. The resulting reaction mixture was analyzed by gas chromatography to confirm that 2-mesityl-2-propanol and α-methyl-2,4,6-trimethylstyrene were obtained in a yield of 66.8% and 14.7%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07494962B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-976627a1337f4ce79806db3ae29f0739 |
| Source note | uspto-grants-2009_02 |