HRID1726904

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10476

Cyanogen bromide

CBrN

HCID18373882

N1-(2-Methoxyethyl)-1,2-ethanediamine

C5H14N2O

PRODUCTS

生成物

HCID69026589

未命名化合物

收率 88.8%

PROCEDURE

实验过程

Reaction of N-(2-methoxyethyl)ethylenediamine (16.0 g, 0.135 mol) (R. C. F. Jones and J. R. Nichols, Tetrahedron Lett., 1990, 31, 1767-1770) with cyanogen bromide (14.34 g, 0.135 mol) as described in the preparation of intermediate 6 gave 26.86 g (88% yield) of the title product as large white prisms (ethanol); mp 143-145° C.