HCID 57566928, compound → HCID 57567009, compound

Participants

Reaction Steps

To a solution of 29 (0.9 g, 2.26 mmol) in EtOH (15 mL) was added 10% Pd/C. The solution was then placed under vacuum and recharged with H2. The reaction mixture was stirred under H2 overnight. After filtration and removal of solvent, the residue was placed under vacuum for 10 h to give 30. Etherification of 30 was performed as set forth in Example 27.

Provenance & Evidence