HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[4-(3-Acetoxy-1-butenyl)phenyl]-5-trimethylsilyloxy-pyridine → 2-[4-(3-Acetoxy-1-butyl)phenyl]-5-trimethylsilyloxy-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[4-(3-Acetoxy-1-butenyl)phenyl]-5-trimethylsilyloxy-pyridine | HCID 54198349 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-[4-(3-Acetoxy-1-butyl)phenyl]-5-trimethylsilyloxy-pyridine | HCID 19017251 | 85.2% |
Reaction Steps
14 g of 2-[4-(3-acetoxy-1-butenyl)phenyl]-5-trimethylsilyloxy-pyridine, 2 g of palladium on active charcaol (10 wt. %) and 200 ml of tetrahydrofuran are hydrogenated in an analogous manner to Example 1(a) to give 12 g of 2-[4-(3-acetoxy-1-butyl)phenyl]-5-trimethylsilyloxy-pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326497 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-56b38fed244c4848b6b315f28d65a503 |
| Source note | uspto-grants-1994_07 |