Benzoyl Peroxide → HCID 19018243, compound

HRID 1728445Notes

Reaction equation

HRID 1728445 reaction equation
[CH3:1][C:2]1([CH2:8][O:9][C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[Br:17]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[CH3:1][C:2]1([CH2:8][O:9][C:10]2[CH:11]=[CH:12][C:13]([CH2:16][Br:17])=[CH:14][CH:15]=2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Participants

5

Reactant 3

HCID 7187Benzoyl PeroxideHCID 67184N-bromobutanimideHCID 18960946HCID 18960946, compound

Product 1

HCID 19018243HCID 19018243, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

A solution of 2.2 g (10 mmol) of 4-[((1-methyl)cyclohexyl)methoxy]toluene, 1.8 g (10 mmol) of N-bromosuccinimide and 0.02 g of benzoyl peroxide in 60 ml of carbon tetrachloride was refluxed for 16 hours. The reaction was cooled to room temperature, filtered and the filtrate evaporated to give the product which was used without further purification.

Workup

  1. filtrationfiltered
  2. customthe filtrate evaporated
  3. customto give the product which
  4. customwas used without further purification

Sources & evidence

ORD record
ord-ca0abe3162c0455da3dcada0f7ba6584
Source dataset
uspto-grants-1994_07
Patent number
US05326905

Reaction notes

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