HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 5-Phenyl-2,4-pentadienoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Styrene | HCID 7501 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-Phenyl-2,4-pentadienoic acid | HCID 73777 | — |
Reaction Steps
Styrene and acrylic acid were dissolved in benzene in a total concentration of 30% by weight. An amount of 0.2% by weight based on the total monomers of azobisisobutyronitrile was added to the solution. The mixture was sealed in a tube under a nitrogen gas, and the polymerization was carried out at 70° C. over a period of 48 hours to provide a styrene-acrylic acid copolymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328795 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-c1fd24e57bb940d28c51c98824965756 |
| Source note | uspto-grants-1994_07 |