HRID1728592
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of the nitroindole (D2) (5 g; 28.4 mM) and 5% palladium on charcoal in ethanol (300 ml) was hydrogenated at 60 p.s.i. (4.14×105Pa) at room temperature for 3 h. Removal of the catalyst by filtration followed by evaporation of the solvent gave the title compound (3.39 g; 95%).
WORKUP
后处理
- customRemoval of the catalyst
- filtrationby filtration
- customfollowed by evaporation of the solvent