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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1728648Generated: November 1, 2026

1-Chloroethyl chloroformate → HCID 131718534, compound

https://huagongshe.com/reaction/1728648

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Chloroethyl chloroformateHCID 521305—
ReactantHCID 131718535HCID 131718535—
Solvent1,2-DichloroethaneHCID 11—
ProductHCID 131718534HCID 13171853464.7%

Reaction Steps

Was prepared from compound (1) (2.4 g) by treatment with 1-chloroethyl chloroformate (1.02 g) in 1,2-dichloroethane (100 ml) as described by Olofson et. al (J. Org. Chem. 49 (1984) 2081). Rinse up on a silica gel column gave 1.5 g of compound (6). M.p. 95°-100° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05328917
Source datasetuspto-grants-1994_07
ORD IDord-6a6038daf2af422283fed0c2ebaa3bd2
Source noteuspto-grants-1994_07