HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 131718544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sesamol | HCID 68289 | — |
| Reactant | HCID 53871722 | HCID 53871722 | — |
| Reactant | HCID 131718543 | HCID 131718543 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131718544 | HCID 131718544 | — |
Reaction Steps
Was prepared from the crude 1-(2-methylbutyl)-analogue of (18) (3.8 g), NaH (0.81 g) and sesamol (2.13 g) in DMF (50 ml) as described for compound (17). The crude product was purified several times on a silica gel column using ethylacetate and heptane/ether 4/1 as eluents. Compound (19) was identified by 1H NMR and MS. M.p. 238.5°-239.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328917 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-e3630293168e47eab9ee1adb5e7be810 |
| Source note | uspto-grants-1994_07 |