Methyl iodide → 131988-13-1

HRID 1728670Notes

Reaction equation

HRID 1728670 reaction equation
[CH3:1][I:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:6][C:7]1[C:8]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180132HCID 15180132, compound

Product 1

HCID 15819045131988-13-1

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.37 ml, 6 mmol) and 3-(4-propoxy-1,2,5-thiadiazol-3-yl )pyridine (700 rag, 3.1 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.98 g (88%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.98 g (88%)

Sources & evidence

ORD record
ord-394225d5f04f4f629afcdf83a5989007
Source dataset
uspto-grants-1994_07
Patent number
US05328925

Reaction notes

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