Methyl iodide → 3-(3-Pentyloxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 1728677Notes

Reaction equation

HRID 1728677 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 151801343-(3-Pentyloxy-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190755023-(3-Pentyloxy-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-pentyloxy-1,2,5-thiadiazol-3-yl)pyridine (620 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.81 g (84%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.81 g (84%)

Sources & evidence

ORD record
ord-2d940dfe2b1a48e29944acfe25fd6a10
Source dataset
uspto-grants-1994_07
Patent number
US05328925

Reaction notes

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