Methyl iodide → HCID 19075363, compound

HRID 1728681Notes

Reaction equation

HRID 1728681 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075319HCID 19075319, compound

Product 1

HCID 19075363HCID 19075363, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 10 mmol) and 3-(4-isopentyloxy-1,2,5-thiadiazol-3-yl)pyridine (622 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.78 g (81%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.78 g (81%)

Sources & evidence

ORD record
ord-3d8c80a0ab2f477584a52a0f6f9a6fcd
Source dataset
uspto-grants-1994_07
Patent number
US05328925

Reaction notes

Loading…