Methyl iodide → HCID 19075279, compound
Reaction equation
[CH3:1][I:2].[Cl:3][C:4]1[C:5]([C:9]2[CH:10]=[N:11][CH:12]=[CH:13][CH:14]=2)=[N:6][O:7][N:8]=1>CC(C)=O>[I-:2].[Cl:3][C:4]1[C:5]([C:9]2[CH:10]=[N+:11]([CH3:1])[CH:12]=[CH:13][CH:14]=2)=[N:6][O:7][N:8]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(4-chloro-1,2,5-oxadiazol-3-yl)pyridine (230 mg, 1.2 mmol) in acetone. The reaction mixture was stirred at room temperature for 18 h and evaporated to give the title compound.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-447d16007daf435ebb855c6f9fec7c87
- Source dataset
- uspto-grants-1994_07
- Patent number
- US05328925
Reaction notes
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