HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 3-(Tetradecyloxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Methyl 3-(tetradecyloxy)benzoate | HCID 5152765 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(Tetradecyloxy)benzoic acid | HCID 3262311 | 93.1% |
Reaction Steps
The title compound is prepared by the procedure of Example 2 using 234 g of 3-(tetradecyloxy)benzoic acid methyl ester, 113.0 g of potassium hydroxide, 1 L of methyl alcohol and 120 ml of water. The solid residue is recrystallized from methyl alcohol/ethyl alcohol to give 209 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-11e6432a34374faf8656e7f8be781153 |
| Source note | uspto-grants-1994_07 |