HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → 1-(Bromomethyl)-3-(tetradecyloxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | 3-(Tetradecyloxy)benzenemethanol | HCID 10041710 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-(Bromomethyl)-3-(tetradecyloxy)benzene | HCID 9977250 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 20 using 2.5 g of product from Example 24, 10 ml acetonitrile, 0.339 g of pyridine and 2.11 g of phosphorus tribromide. The product, 2.27 g, is obtained as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-f7937b16c2344fb6b94fb9dc6ddf0503 |
| Source note | uspto-grants-1994_07 |