HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 19015591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | N-(pyridin-2-ylmethyl)acetamide | HCID 5084090 | — |
| Reactant | 3-Chloro-4-(tetradecyloxy)benzoyl chloride | HCID 19016288 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19015591 | HCID 19015591 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 27 using 1.31 g of product from Example 38, 0.535 g of product from Example 12, 0.171 g of washed 50% sodium hydride and 12 ml of tetrahydrofuran. The residue is purified by column chromatography (silica gel:35% ethyl acetate/hexane) to give 0.067 g of product as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-dc68493e227f4516a9a3169ca15535b7 |
| Source note | uspto-grants-1994_07 |