HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Methoxy-4-(tetradecyloxy)benzeneacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 3-Methoxy-4-(tetradecyloxy)benzeneacetic acid ethyl ester | HCID 53766224 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Methoxy-4-(tetradecyloxy)benzeneacetic acid | HCID 19014799 | 68% |
Reaction Steps
The title compound is prepared by the procedure of Example 64 using 60 g of product from Example 66, 24.84 g Of potassium hydroxide, 45 ml of water and 650 ml of ethyl alcohol. The reaction is heated at reflux temperature for 41 hours. The residue is recrystallized from methylene chloride/hexane to give 38 g of the desired product as cream needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-5a247f7fb5234b01a98218a7aa711bcf |
| Source note | uspto-grants-1994_07 |