HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19015379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(Decyloxy)-3-(1,1-dimethylethyl)benzoic acid methyl ester | HCID 53926307 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19015379 | HCID 19015379 | 90.3% |
Reaction Steps
A mixture of 15.0 g of product from Example 130. 7.24 g of potassium hydroxide, 100 ml methyl alcohol, 40 ml ethyl alcohol and 10 ml of water is heated at reflux temperature for 18 hours. The reaction is cooled to room temperature, made acidic to pH 2, concentrated in vacuo, swirled with water and the solid collected. The solid residue is washed with water and dried in a vacuum oven to give 13 g of the desired product as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05328921 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-e358a79a6a6e4b898052d0582a65b449 |
| Source note | uspto-grants-1994_07 |