Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19015330 | HCID 19015330 | — |
| Product | HCID 19016445 | HCID 19016445 | 99.3% |
Reaction Steps
A mixture of 0.80 g of product from Example 146 and 11.34 g of methyl iodide is heated, in a sealed tube, at 100° C. for 10 hours. The reaction is concentrated in vacuo to give 1.02 g of the desired product as light yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05328921 |
|---|
| Source dataset | uspto-grants-1994_07 |
|---|
| ORD ID | ord-0d86e845d15349afb4aac2e23bed0395 |
|---|
| Source note | uspto-grants-1994_07 |
|---|
