HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13451547, compound → HCID 22846170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13451547 | HCID 13451547 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22846170 | HCID 22846170 | 98.2% |
Reaction Steps
1.18 g of (3S, 4R)-3-methoxycarbonyl-4-methylcyclopentanone was dissolved in 20 ml of 3N-HCl, and the solution was refluxed for 2 hours. The reaction mixture was allowed to stand to return to room temperature, and concentrated. The residue was concentrated under a reduced pressure, and thus 1.05 g of the titled compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05329042 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-97db591f08eb41cca719ab1c3ddb7cea |
| Source note | uspto-grants-1994_07 |