HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 88424876, compound → HCID 131718558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 88424876 | HCID 88424876 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 131718558 | HCID 131718558 | 100% |
Reaction Steps
A mixture of 12.0 g (55 mmol) of (E)-2-methyl-4-[(1S,2R,3S,5S)-3-pinanyl]-2-butenal, 100 ml of hexane and 0.36 g of 5% palladium on charcoal is hydrogenated for 3 h. at atmospheric pressure. After filtration of the catalyst and evaporation of the solvent under vacuum there are obtained 12.2 g of (R/S)-2-methyl-4-[(1S,2R,3S,5S)-3-pinanyl]butanal (yield=100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05329052 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-24ac9ee79e3b4569b96fd201b245e3d3 |
| Source note | uspto-grants-1994_07 |