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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1728994Generated: November 1, 2026

HCID 88424876, compound → HCID 131718558, compound

https://huagongshe.com/reaction/1728994

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 88424876HCID 88424876—
CatalystPalladiumHCID 23938—
SolventHexaneHCID 8058—
ProductHCID 131718558HCID 131718558100%

Reaction Steps

A mixture of 12.0 g (55 mmol) of (E)-2-methyl-4-[(1S,2R,3S,5S)-3-pinanyl]-2-butenal, 100 ml of hexane and 0.36 g of 5% palladium on charcoal is hydrogenated for 3 h. at atmospheric pressure. After filtration of the catalyst and evaporation of the solvent under vacuum there are obtained 12.2 g of (R/S)-2-methyl-4-[(1S,2R,3S,5S)-3-pinanyl]butanal (yield=100%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05329052
Source datasetuspto-grants-1994_07
ORD IDord-24ac9ee79e3b4569b96fd201b245e3d3
Source noteuspto-grants-1994_07