Thionyl Chloride → HCID 54264694, compound

HRID 1729001Notes

Reaction equation

HRID 1729001 reaction equation
S(Cl)([Cl:3])=O.[CH2:5]([O:13][C:14]1[CH:15]=[C:16]([C:26]([OH:28])=O)[C:17]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:18][CH:19]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>>[CH2:5]([O:13][C:14]1[CH:15]=[C:16]([C:26]([Cl:3])=[O:28])[C:17]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:18][CH:19]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 23162226HCID 23162226, compound

Product 1

HCID 54264694HCID 54264694, compound

Procedure

With an excess amount of thionyl chloride, 4.0 g of 4-n-octyloxybiphenyl carboxylic acid was heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-octyloxybiphenyl carboxylic acid chloride.

Workup

  1. temperatureunder refluxing for 6 hours
  2. distillationUnaltered thionyl chloride was distilled off

Sources & evidence

ORD record
ord-04352a1cef794bdfb63b21f8b06aae25
Source dataset
uspto-grants-1994_07
Patent number
US05330678

Reaction notes

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