HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67824325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 9928781 | HCID 9928781 | — |
| Product | HCID 67824325 | HCID 67824325 | — |
Reaction Steps
12.7 g (35.3 mmol) of 2-[[3-[[2-(2-methoxyphenoxy)ethyl]methylamino]propyl]amino]pyrimidine-4-carboxamide and 300 ml of methanol are introduced into a 0.5 l round-bottomedflask, a stream of gaseous hydrochloric acid is passed through for a few minutes and the mixture is heated at the reflux temperature of the methanol for 4 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05330985 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-4a9438649780479cbbda62ea09e10af1 |
| Source note | uspto-grants-1994_07 |