Methyl iodide → HCID 23371647, compound

HRID 1729196Notes

Reaction equation

HRID 1729196 reaction equation
[N:1]1([C:10]2[N:15]=[C:14]([NH:16][CH3:17])[N:13]=[CH:12][N:11]=2)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[CH3:18][I:19]>>[I-:19].[CH3:17][NH:16][C:14]1[N:13]=[CH:12][N+:11]([CH3:18])=[C:10]([N:1]2[C:9]3[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=3)[CH:3]=[CH:2]2)[N:15]=1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 23371657HCID 23371657, compound

Product 1

HCID 23371647HCID 23371647, compoundYield 29%

Procedure

Using a similar process to that described in Example 1, 2-(indol-1-yl)-4-methylamino-1,3,5-triazine was reacted with methyl iodide to afford 4-methylamino-2-(indol-1-yl)-1-methyl-1,3,5-triazinium iodide in 29% yield as a solid, mp 284°-285° C. (after recrystallisation from methanol).

Sources & evidence

ORD record
ord-690f985297014dc0beac5452707e4795
Source dataset
uspto-grants-1994_07
Patent number
US05332737

Reaction notes

Loading…