HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzoic Acid → p-Anisoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzoic Acid | HCID 7478 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | p-Anisoyl chloride | HCID 7477 | — |
Reaction Steps
2 equivalents of thionyl chloride and 0.1 g of aluminum chloride are added to 10 g (0.06 mole) of 4-methoxybenzoic acid in suspension in 60 ml of petroleum ether. This reaction mixture is refluxed for 5 hours. The solution is concentrated under reduced pressure. The residual oil crystallizes in the presence of petroleum ether at 0° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332735 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-b76d3de1b6494f2fa9771400b095919d |
| Source note | uspto-grants-1994_07 |