Ethanol → HCID 19011703, compound

HRID 1729217Notes

Reaction equation

[CH2:1]1[O:19][C:18]2[C:3](=[CH:4][C:5]([N+:20]([O-:22])=[O:21])=[C:6]([CH:17]=2)[C:7]([N:9]2[CH2:13][CH2:12][CH2:11][CH:10]2[C:14]([OH:16])=[O:15])=[O:8])[O:2]1.CO.[CH2:25](O)[CH3:26]>>[CH2:1]1[O:19][C:18]2[C:3](=[CH:4][C:5]([N+:20]([O-:22])=[O:21])=[C:6]([CH:17]=2)[C:7]([N:9]2[CH2:13][CH2:12][CH2:11][CH:10]2[C:14]([O:16][CH2:25][CH3:26])=[O:15])=[O:8])[O:2]1

Participants

Reactant 3

HCID 702Ethanol

HCID 887Methanol

HCID 19011691HCID 19011691, compound

Product 1

HCID 19011703HCID 19011703, compoundYield 85%

Procedure

By carrying out the procedure as in Example 11, but replacing 4-hydroxy-1-(3,4-methylenedioxybenzoyl)pyrrolidine-2-carboxylic acid by 1-(4,5-methylenedioxy-2-nitrobenzoyl)pyrrolidine-2-carboxylic acid and methanol by ethanol, the title product is obtained.

Sources & evidence

ORD record: ord-caaa90451b8b46bc80bdd931a01b3c9e
Source dataset: uspto-grants-1994_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05332735

Reaction notes

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