HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(9-fluorenylcarbonyl)glycine → 2-[[[N-(9-fluorenylcarbonyl)glycyl]-L-valyl]amino]-6-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(9-fluorenylcarbonyl)glycine | HCID 19011682 | — |
| Reactant | 6-methyl-2-(L-valylamino)benzoic acid | HCID 54180568 | — |
| Product | 2-[[[N-(9-fluorenylcarbonyl)glycyl]-L-valyl]amino]-6-methylbenzoic acid | HCID 54195589 | 33.4% |
Reaction Steps
84 mg of 2-[[[N-(9-fluorenylcarbonyl)glycyl]-L-valyl]amino]-6-methylbenzoic acid was prepared exactly as in step c) of Example 3, except that 126 mg of 6-methyl-2-(L-valylamino)benzoic acid was subjected to a condensation reaction with 188 mg of N-(9-fluorenylcarbonyl)glycine in place of 9-fluorenyloxyacetic acid used in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332734 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-af4727b6c65a443582c7c6452f348e17 |
| Source note | uspto-grants-1994_07 |