HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenylacetaldehyde → N-[(E)-p-methoxystyryl]-N-methyl-2-(cyclohexen-1-yl)ethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenylacetaldehyde | HCID 79782 | — |
| Reactant | [2-(Cyclohex-1-en-1-yl)ethyl](methyl)amine | HCID 18360934 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-[(E)-p-methoxystyryl]-N-methyl-2-(cyclohexen-1-yl)ethylamine | HCID 19012968 | 95.3% |
Reaction Steps
The solution of p-methoxyphenylacetaldehyde in 200 ml of toluene, prepared according to Example la), is added under reflux within one hour to a mixture of 78 g (55.5 mmol) of N-methyl-2-(cyclohexen-1-yl)ethylamine in 20 ml of toluene. After 1 hour under reflux there is obtained N-[(E)-p-methoxystyryl]-N-methyl-2-(cyclohexen-1-yl)ethylamine (yield 95.3%) dissolved in toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332821 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-64b5285d28e54bc781d505af73c64263 |
| Source note | uspto-grants-1994_07 |