HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → Diisopropylethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | Diisopropylethylamine | HCID 81531 | — |
Reaction Steps
in the presence of an organic base such as triethylamine or diisopropylethylamine, and an inert organic solvent such as dichloromethane, chloroform or THF, under an inert atmosphere such as argon at a reduced temperature of from about -20° to about 15° C., to form the sulfonamide I of the invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332822 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-ad31b6f19b6942e4984e167a2ce9124c |
| Source note | uspto-grants-1994_07 |