HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 86748028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | HCID 86748029 | HCID 86748029 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 86748028 | HCID 86748028 | — |
Reaction Steps
By the method of Example 1, (E)-(10H,11H-dibenzo-[a,c]cyclohepten-5-ylidene)-2-butenal (1.25 g, 4.8 mmol) was reacted methyl acetoacetate. Chromatography on silica gel (1:4, ethyl a cetate:hexane as eluant) provided title product (0.6 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332857 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-a9c6489b7d1d45599d3c35455d10d816 |
| Source note | uspto-grants-1994_07 |