HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl Alcohol → Allyl 4-hydroxy-2-trifluoromethylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | 4-Hydroxy-2-(trifluoromethyl)benzoic acid | HCID 2775111 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | Allyl 4-hydroxy-2-trifluoromethylbenzoate | HCID 14852524 | 59% |
Reaction Steps
In a manner analogous to Example l(a) starting with 2 g (9.7 mmoles) of 4-hydroxy-2-trifluoromethylbenzoic acid treated at 100° C. for 12 hours with 20 ml of allyl alcohol and 260 μl of concentrated sulfuric acid, give 1.4 g (59% yield) of the expected ester having a melting point of 82°-83°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05332856 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-7139cb40fa3b4670acda5089e342efb4 |
| Source note | uspto-grants-1994_07 |