HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → 4-Ethylamino-3-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 4-Chloro-3-nitrobenzamide | HCID 27942 | — |
| Product | 4-Ethylamino-3-nitrobenzamide | HCID 3708922 | — |
Reaction Steps
II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989522 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-bb3097a7e15a44488e01fcb467723d81 |
| Source note | uspto-grants-1976_11 |