HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Chlorophenyl)-1-phenylprop-2-en-1-one → HCID 12391103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Chlorophenyl)-1-phenylprop-2-en-1-one | HCID 95326 | — |
| Reactant | Carbamimidoyl-acetic acid ethyl ester | HCID 4599837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12391103 | HCID 12391103 | 73% |
Reaction Steps
Upon heating a solution of 24.3 g of 3-chlorobenzylideneacetophenone and 13.0 g of amidinoacetic acid ethyl ester in 250 ml of ethanol for 4 hours, 2-amino-6-phenyl-4-(3-chlorophenyl)-1,4-dihydropyridine-3-carboxylic acid ethyl ester of melting point 161°C is obtained. Yield: 73 percent of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989708 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-fc907ac78f634e459ceb4a6f033d3515 |
| Source note | uspto-grants-1976_11 |